Titanium nitride magnetron sputtering презентация

Preparation Beam tube cleaned according to UHV practices. Vacuum fired at 450 C. Assembled into coating system. Two Fermilab 6” OD tubes in process.

Слайд 1TITANIUM NITRIDE MAGNETRON SPUTTERING
Performed at Brookhaven National Lab
for Fermilab Main Injector


Electron Cloud Studies
June 2009

Linda Valerio
September 11, 2009

Слайд 2Preparation
Beam tube cleaned according to UHV practices.
Vacuum fired at 450 C.
Assembled

into
coating system.



Two Fermilab 6” OD tubes in process.


Слайд 3Coating System
3


Слайд 4Coating System
Overview of system with
two Fermilab tubes.
Gas introduction flange.

Power and

cooling connections.

Слайд 5Titanium Cathode Assembly








Insertion of magnet string into Ti cathode.


Слайд 6The Coating Process
Balance temperature, pressure, flow rate, and voltage to control

deposition.
Start with Argon only for pure Ti layer, then add Nitrogen.
Monitor voltage discharge characteristics, plasma color, and partial pressures on RGA to confirm process.
The Fermilab setup started at 200 C and 4 e-7 Torr and took less than an hour.

Balance tempe
Vacuum fired at 450 C.
Assembled into
coating system.



Argon plasma

Argon + Nitrogen plasma


Слайд 7System Disassembly
Nitrogen insertion tube attached to titanium cathode still inside chamber.
Titanium

cathode with nitrogen distribution tube. Magnet string position indicated by discoloration.

Слайд 8Coating Complete
Coating analysis coupons were inserted
adjacent to production tubes.

Finished Fermilab

tube.

Слайд 9Installed in Main Injector
One coated tube installed during Summer 2009 shutdown

at MI-521.
One uncoated tube also installed, with electron cloud detectors on both.

Слайд 10Current Status
Main Injector startup September 10, 2009 – first opportunity to

start electron cloud studies with coated tube.
Brookhaven will also coat a Main Injector elliptical tube.
Fermilab has a separate collaboration with SLAC to coat a Main Injector elliptical tube using electrostatic sputtering (no magnets).
Eventually, comparison of both methods will be done to determine which is better suited for Main Injector.

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